Singhal, S. K. and Srivastava, A. K. and Pant, R. P. and Gupta, Anil K. and Halder, S. K. and Singh, B. P. and Gupta, Anil K. (2008) Synthesis of boron nitride nanotubes employing mechanothermal process and its characterization. Journal of Materials Science: Materials in Electronics, 43 (15). 5243-5250 . ISSN 0957-4522

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Abstract

Multi-walled boron nitride (BN) nanotubes having cylindrical structure were synthesized employing the mechanothermal process. In this process hexagonal boron nitride powder (hBN) was first ball milled for 50-100 h using a high-energy ball mill and the ball-milled samples were annealed in N(2) atmosphere for about 10 h in the temperature range of 950-1300 degrees C. The BN nanotubes exhibited a well-crystallized hexagonal structure with about 25-40 nm in diameter and up to 1 mu m length. These BN nanotubes were well characterized using various techniques, such as, XRD, SEM, TEM and Raman Spectroscopy.

Item Type: Article
Subjects: Materials Science
Divisions: UNSPECIFIED
Depositing User: Ms Neetu Chandra
Date Deposited: 26 Jul 2017 05:27
Last Modified: 26 Jul 2017 05:27
URI: http://npl.csircentral.net/id/eprint/2151

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